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Babashpour-Asl, Marzieh, Piryaei, Marzieh. (1400). Analysis of Grammosciadium platycarpum Boiss. & Hausskn. Essential Oil Using of Three Dimensional Nanocomposite Based on MgAl Layered Double Hydroxide as a Fiber Coating of SPME. سامانه مدیریت نشریات علمی, 10(2), 161-167. doi: 10.22092/jmpb.2020.351310.1237
Marzieh Babashpour-Asl; Marzieh Piryaei. "Analysis of Grammosciadium platycarpum Boiss. & Hausskn. Essential Oil Using of Three Dimensional Nanocomposite Based on MgAl Layered Double Hydroxide as a Fiber Coating of SPME". سامانه مدیریت نشریات علمی, 10, 2, 1400, 161-167. doi: 10.22092/jmpb.2020.351310.1237
Babashpour-Asl, Marzieh, Piryaei, Marzieh. (1400). 'Analysis of Grammosciadium platycarpum Boiss. & Hausskn. Essential Oil Using of Three Dimensional Nanocomposite Based on MgAl Layered Double Hydroxide as a Fiber Coating of SPME', سامانه مدیریت نشریات علمی, 10(2), pp. 161-167. doi: 10.22092/jmpb.2020.351310.1237
Babashpour-Asl, Marzieh, Piryaei, Marzieh. Analysis of Grammosciadium platycarpum Boiss. & Hausskn. Essential Oil Using of Three Dimensional Nanocomposite Based on MgAl Layered Double Hydroxide as a Fiber Coating of SPME. سامانه مدیریت نشریات علمی, 1400; 10(2): 161-167. doi: 10.22092/jmpb.2020.351310.1237

Analysis of Grammosciadium platycarpum Boiss. & Hausskn. Essential Oil Using of Three Dimensional Nanocomposite Based on MgAl Layered Double Hydroxide as a Fiber Coating of SPME

Journal of Medicinal plants and By-product
دوره 10، شماره 2، آذر 2021، صفحه 161-167    اصل مقاله (524.88 K)
نوع مقاله: Research Paper
شناسه دیجیتال (DOI): 10.22092/jmpb.2020.351310.1237
نویسندگان
Marzieh Babashpour-Asl* 1؛ Marzieh Piryaei2
1Department of Horticulture, Maragheh Branch, Islamic Azad University, Maragheh, Iran
2Department of Chemistry, Faculty of Science, University of Maragheh, Maragheh, Iran
چکیده
This study evaluates the reliability of polystyrene/MgAl-layered double hydroxide as a 3D new nanostructure solid phase microextraction fiber coating for extraction and determination the essential oil of Grammosciadium platycarpum Boiss. & Hausskn. growing wild in Maragheh region, East Azerbaijan province, Iran. The Headspace solid phase microextraction coupled with gas chromatography/mass spectrometric method was applied for analyzing of volatile oils. The Headspace solid phase microextraction parameters including the extraction temperature and time, sample weight, and water amount were optimized. The method was compared with traditional hydrodistillation. The analysis of the oils resulted in the identification of 31 compounds. Linalool (57.31 and 61.05%) and α-humulene (5.62 and 4.82%) were found to be the major components, in hydrodistillation and headspace solid phase microextraction methods, respectively. The novel 3D nanostructure fiber coating based on MgAl LDH had the advantages of the strong interaction between analyte and sorbent, simplicity, high thermal stability and more convenient handling than the other traditional SPME fibers. Although to date, SPME devices have been used mainly in laboratory applications, recent research has been directed towards remote monitoring, particularly for clinical, field environmental and industrial hygiene applications.
کلیدواژه‌ها
Volatile Oil؛ Microextraction؛ LDH؛ Nanomaterial؛ Grammosciadium DC؛ GC/MS
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